9GT3
DTPAA CHIP EXPERIMENT, ID29, X,Y SPACING 25,100
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID29 |
| Synchrotron site | ESRF |
| Beamline | ID29 |
| Temperature [K] | 293 |
| Detector technology | PIXEL |
| Collection date | 2024-01-01 |
| Detector | PSI JUNGFRAU 4M |
| Wavelength(s) | 1.073 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 73.600, 68.800, 75.600 |
| Unit cell angles | 90.00, 105.80, 90.00 |
Refinement procedure
| Resolution | 37.680 - 1.670 |
| R-factor | 0.15207 |
| Rwork | 0.151 |
| R-free | 0.17740 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.745 |
| Data reduction software | CrystFEL |
| Data scaling software | CrystFEL |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0430) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 40.000 | 1.710 |
| High resolution limit [Å] | 1.670 | 1.670 |
| Number of reflections | 84347 | 4217 |
| <I/σ(I)> | 6.8 | 1.1 |
| Completeness [%] | 100.0 | |
| Redundancy | 734 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | BATCH MODE | 293 | PEG 6L. HEPES 7.0 |
