9GNV
Human SENP5 in complex with SUMO1
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-07-07 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9791 |
| Spacegroup name | P 65 2 2 |
| Unit cell lengths | 91.062, 91.062, 146.534 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.860 - 2.180 |
| R-factor | 0.1879 |
| Rwork | 0.184 |
| R-free | 0.25890 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.952 |
| Data reduction software | XDS |
| Data scaling software | SCALA |
| Phasing software | PHASER |
| Refinement software | PHENIX (1.17.1_3660) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.860 | 2.328 |
| High resolution limit [Å] | 2.178 | 2.178 |
| Number of reflections | 14291 | 715 |
| <I/σ(I)> | 9.9 | |
| Completeness [%] | 94.2 | |
| Redundancy | 12.3 | |
| CC(1/2) | 0.996 | 0.619 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 2.1 M Malic Ac., pH 7.0 |
