9GNP

SFX structure of Cydia pomonella granulovirus using aerosol sample injection

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	EUROPEAN XFEL BEAMLINE SPB/SFX
Synchrotron site	European XFEL
Beamline	SPB/SFX
Temperature [K]	293
Detector technology	PIXEL
Collection date	2022-03-24
Detector	AGIPD
Wavelength(s)	2.033
Spacegroup name	I 2 3
Unit cell lengths	100.130, 100.130, 100.130
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	40.880 - 2.300
R-factor	0.1845
Rwork	0.178
R-free	0.23500
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	0.797
Data reduction software	CrystFEL
Data scaling software	CrystFEL
Phasing software	PHASER
Refinement software	PHENIX ((1.21.1-5286_9999: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	40.880	2.480
High resolution limit [Å]	2.300	2.300
Number of reflections	6978	1053
<I/σ(I)>	6.22	0.22
Completeness [%]	92.0	69
Redundancy	761	26
CC(1/2)	0.984	0.121

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	IN CELL		293	In vivo