Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-11-30 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.9998 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 67.747, 100.443, 103.376 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 72.040 - 1.930 |
| R-factor | 0.20035 |
| Rwork | 0.198 |
| R-free | 0.23844 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.491 |
| Data reduction software | autoPROC (1.1.7) |
| Data scaling software | autoPROC ((Version 1.1.7)) |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 72.040 | 1.970 |
| High resolution limit [Å] | 1.930 | 1.930 |
| Number of reflections | 52860 | 2598 |
| <I/σ(I)> | 7.1 | |
| Completeness [%] | 98.9 | 98.8 |
| Redundancy | 7.1 | |
| CC(1/2) | 0.990 | 0.480 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | 2M Calcium Acetate, 100mM Sodium Cacodylate pH 6.50 and 40% PEG 600. |
