9GLO

Crystal Structure of UFC1 C116E&T106S

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-2
Synchrotron site	ESRF
Beamline	ID23-2
Temperature [K]	298
Detector technology	PIXEL
Collection date	2024-01-19
Detector	DECTRIS EIGER X 9M
Wavelength(s)	0.87313
Spacegroup name	P 41 21 2
Unit cell lengths	46.802, 46.802, 144.376
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	39.270 - 1.530
Rwork	0.177
R-free	0.20770
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.013
RMSD bond angle	2.027
Data reduction software	autoPROC
Data scaling software	autoPROC
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	39.270	1.585
High resolution limit [Å]	1.530	1.530
Rmeas	0.025	0.164
Number of reflections	25209	2454
<I/σ(I)>	16.9	4.76
Completeness [%]	100.0	100
Redundancy	2	2
CC(1/2)	1.000	0.963

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.5	293	0.1 M Bis-Tris, pH 5.5, 2 M ammonium sulfate