Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2022-12-20 |
| Detector | DECTRIS PILATUS 200K |
| Wavelength(s) | 1.54187 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 47.200, 47.200, 142.800 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.815 - 1.650 |
| Rwork | 0.203 |
| R-free | 0.23100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.680 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.820 | 1.709 |
| High resolution limit [Å] | 1.650 | 1.650 |
| Rmeas | 0.067 | 0.594 |
| Number of reflections | 20255 | 1959 |
| <I/σ(I)> | 12.61 | 1.61 |
| Completeness [%] | 99.6 | 98.49 |
| Redundancy | 2 | 1.9 |
| CC(1/2) | 0.998 | 0.664 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 9 | 293 | 1.4M Sodium potassium monobasic monohydrate/Potassium phosphate dibasic pH 9.0 |
