9GLJ

Crystal Structure of UFC1 T106A

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ESRF BEAMLINE ID23-1
Synchrotron site	ESRF
Beamline	ID23-1
Temperature [K]	298
Detector technology	PIXEL
Collection date	2022-11-10
Detector	DECTRIS EIGER2 XE CdTe 16M
Wavelength(s)	0.87313
Spacegroup name	P 41 21 2
Unit cell lengths	47.222, 47.222, 142.039
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	33.430 - 1.213
Rwork	0.177
R-free	0.19890
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.016
RMSD bond angle	1.916
Data reduction software	autoPROC
Data scaling software	autoPROC
Refinement software	REFMAC (5.8.0267)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.430	1.256
High resolution limit [Å]	1.213	1.213
Rmeas	0.022	0.345
Number of reflections	49774	4863
<I/σ(I)>	15.16	2.32
Completeness [%]	100.0	100
Redundancy	2	2
CC(1/2)	1.000	0.836

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	0.1M NaCl, 0.1M Bis-Tris pH 6.5, 1.5M Ammonium sulfate.