Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 298 |
| Detector technology | PIXEL |
| Collection date | 2023-03-25 |
| Detector | DECTRIS EIGER2 XE 16M |
| Wavelength(s) | 1.34767 |
| Spacegroup name | P 41 21 2 |
| Unit cell lengths | 47.014, 47.014, 142.729 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.654 - 1.426 |
| Rwork | 0.174 |
| R-free | 0.20800 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.837 |
| Refinement software | REFMAC (5.8.0267) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.654 | 1.451 |
| High resolution limit [Å] | 1.426 | 1.426 |
| Rmeas | 0.029 | 0.817 |
| Number of reflections | 29760 | 1017 |
| <I/σ(I)> | 12.1 | 0.7 |
| Completeness [%] | 96.5 | 68.6 |
| Redundancy | 21.3 | 5 |
| CC(1/2) | 0.999 | 0.333 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 7 | 293 | 1M Ammonium Citrate tribasic pH 7.0, 0.1M Bis-Tris Propane pH 7.0. |
