9GIE

NMDA bound to compound 315

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	DIAMOND BEAMLINE I03
Synchrotron site	Diamond
Beamline	I03
Temperature [K]	100
Detector technology	PIXEL
Collection date	2016-01-17
Detector	DECTRIS PILATUS3 6M
Wavelength(s)	0.9763
Spacegroup name	P 21 21 21
Unit cell lengths	72.448, 78.868, 91.984
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	59.945 - 2.360
Rwork	0.194
R-free	0.26020
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.007
RMSD bond angle	1.498
Data reduction software	autoPROC
Data scaling software	STARANISO
Phasing software	PHASER
Refinement software	REFMAC (5.8.0425)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	91.980	2.400
High resolution limit [Å]	2.360	2.360
Rmerge	0.143	0.823
Number of reflections	22308	1079
<I/σ(I)>	12.8	2.3
Completeness [%]	100.0
Redundancy	6
CC(1/2)	1.000	0.800

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	7.5	282.15	24% PEG 3350 and 0.1 M hepes pH 7.5