9GID

NMDA bound to compound 338

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Collection date	2017-01-04
Detector	RIGAKU SATURN 944
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	41.560, 72.500, 95.790
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	23.960 - 2.000
Rwork	0.206
R-free	0.25980
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.008
RMSD bond angle	1.628
Data reduction software	MOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0430 (refmacat 0.4.82))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	23.960	2.050
High resolution limit [Å]	2.000	2.000
Rmerge	0.171	0.729
Number of reflections	45513	1113
<I/σ(I)>	4.3	0.8
Completeness [%]	95.1
Redundancy	2.4
CC(1/2)	0.974	0.478

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.7	282.15	20% (w/v) PEG 3350, 0.1 M Bis-Tris pH 5.7 and 0.2 M lithium sulfate