9GIC

NMDA bound to compound 345

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU MICROMAX-007 HF
Temperature [K]	100
Detector technology	CCD
Collection date	2017-01-04
Detector	RIGAKU SATURN 944
Wavelength(s)	1.54
Spacegroup name	P 21 21 21
Unit cell lengths	41.960, 70.745, 96.000
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	20.566 - 1.823
Rwork	0.191
R-free	0.22050
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.009
RMSD bond angle	1.656
Data reduction software	MOSFLM
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0430 (refmacat 0.4.82))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	20.570	1.860
High resolution limit [Å]	1.820	1.820
Rmerge	0.114	0.324
Number of reflections	2553444	6489
<I/σ(I)>	10.8	3.7
Completeness [%]	97.5
Redundancy	6
CC(1/2)	0.988	0.910

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	5.7	282.15	20% (w/v) PEG 3350, 0.1 M Bis-Tris pH 5.7 and 0.2 M lithium sulfate