9G8I

Sumo-Darpin-A10-complex

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06DA
Synchrotron site	SLS
Beamline	X06DA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2018-11-09
Detector	DECTRIS PILATUS 2M
Wavelength(s)	1.0
Spacegroup name	P 21 21 21
Unit cell lengths	42.972, 94.747, 120.957
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	44.110 - 2.510
R-factor	0.2486
Rwork	0.243
R-free	0.30150
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.002
RMSD bond angle	0.592
Data reduction software	XDS
Data scaling software	pointless
Phasing software	PHASER
Refinement software	PHENIX ((1.20.1_4487: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	47.370	2.610
High resolution limit [Å]	2.510	2.510
Rmerge	0.097	1.496
Rmeas	0.101	1.558
Rpim	0.028	0.433
Total number of observations	229854	24989
Number of reflections	17608	1948
<I/σ(I)>	17.7	1.7
Completeness [%]	99.9
Redundancy	13.1	12.8
CC(1/2)	1.000	0.897

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP	6.5	293	Bis-Tris pH 6.5, 23% (v/v) PEG 3350