Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-11-14 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | F 2 3 |
| Unit cell lengths | 170.352, 170.352, 170.352 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 19.890 - 3.000 |
| R-factor | 0.2115 |
| Rwork | 0.210 |
| R-free | 0.24280 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.090 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.5) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 28.800 | 14.000 | 3.080 |
| High resolution limit [Å] | 3.000 | 13.420 | 3.000 |
| Rmerge | 0.057 | 0.029 | 2.662 |
| Rmeas | 0.058 | 0.030 | 2.727 |
| Number of reflections | 8328 | 97 | 611 |
| <I/σ(I)> | 32.61 | ||
| Completeness [%] | 99.8 | ||
| Redundancy | 20 | ||
| CC(1/2) | 1.000 | 1.000 | 0.638 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294 | 10 % PEG8000, LITHIUM SULPHATE 0.5M |
