9FZK
SARS CoV-2 nsp10 in complex with theExoN domain from nsp14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | MAX IV BEAMLINE BioMAX |
Synchrotron site | MAX IV |
Beamline | BioMAX |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-12-05 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.976 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 43.935, 100.086, 51.231 |
Unit cell angles | 90.00, 114.59, 90.00 |
Refinement procedure
Resolution | 42.240 - 1.300 |
R-factor | 0.1618 |
Rwork | 0.161 |
R-free | 0.18510 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.014 |
RMSD bond angle | 1.387 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 56.000 | 1.350 |
High resolution limit [Å] | 1.300 | 1.300 |
Rmerge | 0.055 | 0.816 |
Number of reflections | 99531 | 4948 |
<I/σ(I)> | 18.4 | 2.4 |
Completeness [%] | 99.9 | |
Redundancy | 6.9 | |
CC(1/2) | 0.990 | 0.789 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 293 | 0.04-0.24 M Amino acids, 0.1 M buffer system 2 (pH 7.5), 16-38% v/v precipitant mix 2 |