9FXN
Human mitochondrial nuclease EXOG (hEXOG)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | PETRA III, DESY BEAMLINE P11 |
Synchrotron site | PETRA III, DESY |
Beamline | P11 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2023-10-03 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.03326 |
Spacegroup name | P 1 21 1 |
Unit cell lengths | 73.550, 83.560, 74.390 |
Unit cell angles | 90.00, 113.51, 90.00 |
Refinement procedure
Resolution | 40.550 - 1.620 |
R-factor | 0.1587 |
Rwork | 0.157 |
R-free | 0.22800 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.005 |
RMSD bond angle | 0.842 |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 40.550 | 1.720 |
High resolution limit [Å] | 1.620 | 1.620 |
Number of reflections | 97632 | 97632 |
<I/σ(I)> | 1.01 | 1.01 |
Completeness [%] | 93.0 | 93 |
Redundancy | 6.64 | |
CC(1/2) | 0.990 | 0.990 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 291.15 | 16.5 % PEG 8000, 0.1 M Tris-HCL, 0.3 M magnesium chloride hexahydrate |