9FTA

Crystal structure of d(GGGGTTTTGGGG) with Zn and K

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	ELETTRA BEAMLINE 5.2R
Synchrotron site	ELETTRA
Beamline	5.2R
Temperature [K]	294
Detector technology	PIXEL
Collection date	2022-08-01
Detector	DECTRIS PILATUS 2M
Wavelength(s)	2
Spacegroup name	P 21 21 21
Unit cell lengths	26.457, 47.925, 96.076
Unit cell angles	90.00, 89.92, 90.06

Refinement procedure

Resolution	48.038 - 2.490
Rwork	0.334
R-free	0.42580
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.005
RMSD bond angle	1.175
Data reduction software	XDS
Data scaling software	XSCALE
Phasing software	PHASER
Refinement software	REFMAC (5.8.0253)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	48.040	2.554
High resolution limit [Å]	2.490	2.490
Number of reflections	4651	4043
<I/σ(I)>	1.11
Completeness [%]	91.1
Redundancy	4
CC(1/2)	0.891	0.891

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, HANGING DROP		294	30mM NaCaCo(pH6.8), 50mM KCl, 10mM ZnCl2, 2mM Spermine, 5%MPD