Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE ID30B |
| Synchrotron site | ESRF |
| Beamline | ID30B |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2017-08-25 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.976 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 46.749, 134.590, 145.081 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.500 - 2.060 |
| R-factor | 0.28 |
| Rwork | 0.279 |
| R-free | 0.31500 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.070 |
| Data scaling software | xia2 |
| Phasing software | MOLREP |
| Refinement software | BUSTER (2.11.7 PACIOREK) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 44.500 | 2.110 |
| High resolution limit [Å] | 2.060 | 2.060 |
| Rmeas | 0.167 | 2.470 |
| Number of reflections | 54806 | 3234 |
| <I/σ(I)> | 4.38 | |
| Completeness [%] | 94.7 | |
| Redundancy | 4.02 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 13-18% PEG3350 0.2-0.35M Am. Cit. pH7.0 |
