9FLB

Crystal structure of haspin (GSG2) in complex with MU1464

This is a non-PDB format compatible entry.

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	SLS BEAMLINE X06SA
Synchrotron site	SLS
Beamline	X06SA
Temperature [K]	100
Detector technology	PIXEL
Collection date	2019-11-16
Detector	DECTRIS EIGER X 16M
Wavelength(s)	1.00004
Spacegroup name	P 21 21 21
Unit cell lengths	77.750, 79.064, 80.142
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	45.630 - 2.500
R-factor	0.19523
Rwork	0.193
R-free	0.24487
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.177
Data reduction software	XDS
Data scaling software	Aimless
Phasing software	PHASER
Refinement software	REFMAC (5.8.0258)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	45.630	2.590
High resolution limit [Å]	2.500	2.500
Rmerge	0.077	1.017
Rmeas	0.085	1.093
Rpim	0.033	0.436
Number of reflections	17626	1706
<I/σ(I)>	11.7	1.7
Completeness [%]	99.7
Redundancy	6.2	6.2
CC(1/2)	0.998	0.699

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	VAPOR DIFFUSION, SITTING DROP		277	57% MPD, 0.1M MMT 6.0