9FKU
Crystal Structure of AimR from Katmira phage
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALBA BEAMLINE XALOC |
| Synchrotron site | ALBA |
| Beamline | XALOC |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2024-05-30 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97918 |
| Spacegroup name | C 2 2 21 |
| Unit cell lengths | 69.765, 203.582, 143.069 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 48.690 - 1.900 |
| R-factor | 0.17999 |
| Rwork | 0.178 |
| R-free | 0.21206 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | autoPROC |
| Data scaling software | Aimless |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.640 | 1.970 |
| High resolution limit [Å] | 1.900 | 1.900 |
| Number of reflections | 80454 | 7816 |
| <I/σ(I)> | 16.2 | 1.7 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 6 | 6.3 |
| CC(1/2) | 0.999 | 0.664 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 294 | 15% pentaeritritol ethoxilate, 3% jeffamine, 0.2M Potassium Acetate, 0.1M MES |
