Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 200 |
| Detector technology | PIXEL |
| Collection date | 2019-02-08 |
| Detector | DECTRIS PILATUS 2M-F |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 61 2 2 |
| Unit cell lengths | 110.103, 110.103, 129.819 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.680 - 1.592 |
| Rwork | 0.148 |
| R-free | 0.19160 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.617 |
| Data reduction software | MOSFLM |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.680 | 1.620 |
| High resolution limit [Å] | 1.590 | 1.590 |
| Rmerge | 0.180 | |
| Rmeas | 0.184 | |
| Rpim | 0.040 | |
| Number of reflections | 61843 | 2977 |
| <I/σ(I)> | 21.3 | |
| Completeness [%] | 99.1 | |
| Redundancy | 39.7 | 38.8 |
| CC(1/2) | 1.000 | 0.543 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 1.2 M Na3Citrate, 0.1M Tris 7.5 |
