Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-09-10 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.00001 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 52.792, 74.768, 68.609 |
| Unit cell angles | 90.00, 102.69, 90.00 |
Refinement procedure
| Resolution | 49.920 - 1.410 |
| R-factor | 0.15806 |
| Rwork | 0.157 |
| R-free | 0.18319 |
| Structure solution method | FOURIER SYNTHESIS |
| RMSD bond length | 0.010 |
| RMSD bond angle | 1.527 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | REFMAC |
| Refinement software | REFMAC (5.8.0232) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 49.920 | 1.530 |
| High resolution limit [Å] | 1.410 | 1.410 |
| Rmeas | 0.063 | 0.676 |
| Number of reflections | 75180 | 3759 |
| <I/σ(I)> | 8.2 | 1.8 |
| Completeness [%] | 86.1 | 34.7 |
| Redundancy | 3.3 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.35M KSCN 28% PEG 3350 |
