9FCE
BelI in complex with SAM from Streptomyces sp. UCK14
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SLS BEAMLINE X06SA |
Synchrotron site | SLS |
Beamline | X06SA |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-04-07 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 1.0 |
Spacegroup name | F 2 2 2 |
Unit cell lengths | 81.430, 165.000, 165.670 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 30.000 - 1.950 |
R-factor | 0.17234 |
Rwork | 0.170 |
R-free | 0.20748 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.004 |
RMSD bond angle | 1.133 |
Data reduction software | XDS |
Data scaling software | XSCALE |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 30.000 | 2.050 |
High resolution limit [Å] | 1.950 | 1.950 |
Rmerge | 0.042 | 0.573 |
Number of reflections | 38727 | 21464 |
<I/σ(I)> | 15.9 | 2.2 |
Completeness [%] | 95.1 | 97.4 |
Redundancy | 3.9 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293 | 0.2 M LiCl, 0.1 M TRIS, 20% PEG 8000 |