Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | DIAMOND BEAMLINE I03 |
| Synchrotron site | Diamond |
| Beamline | I03 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-07-08 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.97622 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 70.574, 75.144, 83.011 |
| Unit cell angles | 90.00, 90.20, 90.00 |
Refinement procedure
| Resolution | 55.710 - 2.020 |
| R-factor | 0.2264 |
| Rwork | 0.225 |
| R-free | 0.26160 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.950 |
| Data reduction software | XDS |
| Data scaling software | XDS |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 55.680 | 2.070 |
| High resolution limit [Å] | 2.020 | 2.020 |
| Number of reflections | 56806 | 4183 |
| <I/σ(I)> | 4.3 | |
| Completeness [%] | 99.8 | |
| Redundancy | 3.3 | |
| CC(1/2) | 0.973 | 0.273 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293 | 20 % PEG3350, pH 5.5 |
