9F9J

Laser excitation effects on BR: Extrapolated 10ps Light dataset recorded at 1281 GW/cm2 at SACLA (+100ps, 1ns, 10ns)

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	SACLA BEAMLINE BL3
Synchrotron site	SACLA
Beamline	BL3
Temperature [K]	293
Detector technology	CCD
Collection date	2017-07-30
Detector	MPCCD
Wavelength(s)	1.227
Spacegroup name	P 63
Unit cell lengths	62.950, 62.950, 111.700
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	16.020 - 1.760
R-factor	0.2432
Rwork	0.239
R-free	0.28200
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.003
RMSD bond angle	0.886
Data reduction software	CrystFEL (0.9.1)
Data scaling software	CrystFEL (0.9.1)
Refinement software	PHENIX ((1.20_4459: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	31.160	1.700
High resolution limit [Å]	1.650	1.650
Number of reflections	29412	2913
<I/σ(I)>	8.2	1.14
Completeness [%]	100.0
Redundancy	425

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIPIDIC CUBIC PHASE		293	0.1M Na/K phosphate pH5.4, 30% PEG 2000