9F9I

Laser excitation effects on BR: Dark dataset recorded at SACLA

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	FREE ELECTRON LASER
Source details	SACLA BEAMLINE BL3
Synchrotron site	SACLA
Beamline	BL3
Temperature [K]	293
Detector technology	CCD
Collection date	2017-07-30
Detector	MPCCD
Wavelength(s)	1.227
Spacegroup name	P 63
Unit cell lengths	62.450, 62.450, 111.170
Unit cell angles	90.00, 90.00, 120.00

Refinement procedure

Resolution	31.230 - 1.600
R-factor	0.1518
Rwork	0.150
R-free	0.17850
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.182
Data reduction software	CrystFEL (0.9.1)
Data scaling software	CrystFEL (0.9.1)
Refinement software	PHENIX ((1.20_4459: ???))

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	31.230	1.640
High resolution limit [Å]	1.590	1.590
Number of reflections	32843	3272
<I/σ(I)>	15.9	1.19
Completeness [%]	100.0	100
Redundancy	1944

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	LIPIDIC CUBIC PHASE	5.6	294	100 mM Na/K Phosphate buffer pH 5.6 30 % PEG 2000