9F9C
Laser excitation effects on BR: Reprocessed Extrapolated 16 ns Light dataset recorded at 0.04 GW/cm2 from Nango et al.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | FREE ELECTRON LASER |
| Source details | SACLA BEAMLINE BL3 |
| Synchrotron site | SACLA |
| Beamline | BL3 |
| Temperature [K] | 293 |
| Detector technology | CCD |
| Collection date | 2016-02-04 |
| Detector | MPCCD |
| Wavelength(s) | 1.63 |
| Spacegroup name | P 63 |
| Unit cell lengths | 62.950, 62.950, 111.700 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 15.740 - 2.000 |
| R-factor | 0.2167 |
| Rwork | 0.212 |
| R-free | 0.25910 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.792 |
| Data reduction software | CrystFEL (0.9.1) |
| Data scaling software | CrystFEL (0.9.1) |
| Refinement software | PHENIX ((1.20_4459: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 38.920 | 2.000 |
| High resolution limit [Å] | 1.950 | 1.950 |
| Number of reflections | 18140 | 1820 |
| <I/σ(I)> | 12.5 | 1.111 |
| Completeness [%] | 100.0 | 100 |
| Redundancy | 369 | 64 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | LIPIDIC CUBIC PHASE | 293 | 0.1M Na/K phosphate pH5.4, 30% PEG 2000 |
