9F81
Crystal structure of RIOK2 with a covalent compound GCL 47
This is a non-PDB format compatible entry.
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06DA |
| Synchrotron site | SLS |
| Beamline | X06DA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-03-24 |
| Detector | DECTRIS PILATUS 2M |
| Wavelength(s) | 0.9184 |
| Spacegroup name | P 32 |
| Unit cell lengths | 65.177, 65.177, 180.349 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 47.890 - 3.020 |
| R-factor | 0.2167 |
| Rwork | 0.214 |
| R-free | 0.28150 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.006 |
| RMSD bond angle | 1.506 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 47.890 | 3.200 |
| High resolution limit [Å] | 3.020 | 3.020 |
| Number of reflections | 16922 | 2723 |
| <I/σ(I)> | 11.3 | 1.3 |
| Completeness [%] | 99.8 | 98.9 |
| Redundancy | 10.5 | 10.6 |
| CC(1/2) | 0.998 | 0.578 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 293.15 | 20% PEG8000, 0.2M magnesium acetate, 0.1M cacodylate pH 6.5 |
