9F3Z
Psychrophilic laccase (multicopper oxidase) from Oenococcus oeni 229 with Histag
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 180 |
Detector technology | PIXEL |
Collection date | 2021-12-09 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.97918 |
Spacegroup name | I 1 2 1 |
Unit cell lengths | 106.050, 56.690, 182.296 |
Unit cell angles | 90.00, 92.87, 90.00 |
Refinement procedure
Resolution | 93.610 - 3.500 |
R-factor | 0.21008 |
Rwork | 0.208 |
R-free | 0.25727 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.003 |
RMSD bond angle | 1.044 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0419) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 93.610 | 3.830 |
High resolution limit [Å] | 3.500 | 3.500 |
Rmerge | 0.452 | 1.230 |
Rmeas | 0.490 | 1.333 |
Rpim | 0.187 | 0.510 |
Total number of observations | 93984 | 22297 |
Number of reflections | 13988 | 3318 |
<I/σ(I)> | 4.8 | 2 |
Completeness [%] | 99.9 | |
Redundancy | 6.7 | 6.7 |
CC(1/2) | 0.973 | 0.717 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 294 | 50% MPD |