Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2014-09-08 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 61.870, 95.160, 69.470 |
| Unit cell angles | 90.00, 115.76, 90.00 |
Refinement procedure
| Resolution | 48.080 - 1.590 |
| R-factor | 0.17551 |
| Rwork | 0.174 |
| R-free | 0.21167 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.530 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | MOLREP |
| Refinement software | REFMAC (5.8.0352) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.080 | 1.630 |
| High resolution limit [Å] | 1.590 | 1.590 |
| Rmerge | 0.086 | |
| Rmeas | 0.093 | |
| Number of reflections | 95818 | 3412 |
| <I/σ(I)> | 14.1 | |
| Completeness [%] | 98.6 | |
| Redundancy | 6.7 | |
| CC(1/2) | 0.999 | 0.836 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 277.15 | 50%pentaerythriol propoxylate 0.1 M Tris, pH 8.0 |
