Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-3 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-3 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2023-02-16 |
| Detector | DECTRIS EIGER X 4M |
| Wavelength(s) | 1.17 |
| Spacegroup name | I 2 2 2 |
| Unit cell lengths | 118.438, 179.767, 234.461 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 71.670 - 3.360 |
| R-factor | 0.201 |
| Rwork | 0.199 |
| R-free | 0.23440 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.430 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 117.230 | 3.490 |
| High resolution limit [Å] | 3.340 | 3.340 |
| Number of reflections | 36015 | 3939 |
| <I/σ(I)> | 0.995 | |
| Completeness [%] | 98.2 | 89.2 |
| Redundancy | 13.5 | 12.5 |
| CC(1/2) | 0.995 | 0.357 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 6.5 | 293 | 1.2 M Sodium Tartrate, 0.1 M ADA, pH 6.5 |
