9EZ2
Vitamin D receptor complex with 1,4b,25-trihydroxyvitamin D3
This is a non-PDB format compatible entry.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SOLEIL BEAMLINE PROXIMA 2 |
Synchrotron site | SOLEIL |
Beamline | PROXIMA 2 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-07-08 |
Detector | DECTRIS EIGER X 9M |
Wavelength(s) | 0.98 |
Spacegroup name | P 65 2 2 |
Unit cell lengths | 66.140, 66.140, 263.740 |
Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
Resolution | 47.990 - 1.800 |
R-factor | 0.2035 |
Rwork | 0.202 |
R-free | 0.23010 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.006 |
RMSD bond angle | 0.785 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHENIX |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 47.990 | 1.864 |
High resolution limit [Å] | 1.800 | 1.800 |
Number of reflections | 32871 | 3184 |
<I/σ(I)> | 23.45 | |
Completeness [%] | 99.3 | |
Redundancy | 2 | |
CC(1/2) | 1.000 | 0.915 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M MES pH 6.0,2.5 M NaOAc |