9ETN
Crystal structure of murine CRTAC1
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-08-06 |
Detector | DECTRIS EIGER2 X 9M |
Wavelength(s) | 0.6702 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 167.514, 84.204, 59.718 |
Unit cell angles | 90.00, 102.70, 90.00 |
Refinement procedure
Resolution | 81.707 - 1.584 |
Rwork | 0.150 |
R-free | 0.19460 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.298 |
Data reduction software | autoPROC |
Data scaling software | STARANISO |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0405) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 81.707 | 1.786 |
High resolution limit [Å] | 1.582 | 1.582 |
Rmerge | 0.086 | 0.777 |
Rmeas | 0.099 | 0.885 |
Rpim | 0.042 | 0.409 |
Number of reflections | 54952 | 2748 |
<I/σ(I)> | 10.9 | |
Completeness [%] | 86.5 | 67.9 |
Redundancy | 4.9 | 4.1 |
CC(1/2) | 0.998 | 0.667 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 5 | 293 | 100 mM sodium-malonate pH 5.0, 12% PEG3350 |