Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X10SA |
| Synchrotron site | SLS |
| Beamline | X10SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-08-26 |
| Detector | DECTRIS EIGER2 X 16M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 107.240, 107.290, 98.430 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 44.730 - 1.200 |
| R-factor | 0.1638 |
| Rwork | 0.163 |
| R-free | 0.18550 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.250 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
| Overall | Inner shell | Outer shell | |
| Low resolution limit [Å] | 50.000 | 50.000 | 1.300 |
| High resolution limit [Å] | 1.200 | 12.000 | 1.200 |
| Rmerge | 0.096 | 0.026 | 2.869 |
| Rmeas | 0.105 | 0.029 | 3.142 |
| Number of reflections | 349643 | 405 | 72691 |
| <I/σ(I)> | 9.94 | ||
| Completeness [%] | 99.3 | ||
| Redundancy | 6.5 | ||
| CC(1/2) | 0.999 | 0.998 | 0.599 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 6.5 | 293 | PEP 629, MES pH 6.5, MgCl2 |
