9EQN
N-terminal domain of Infectious Bursal Disease Virus (IBDV) VP3
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ESRF BEAMLINE MASSIF-3 |
| Synchrotron site | ESRF |
| Beamline | MASSIF-3 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2015-04-21 |
| Detector | DECTRIS PILATUS3 2M |
| Wavelength(s) | 0.9677 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 48.670, 55.761, 52.894 |
| Unit cell angles | 90.00, 110.10, 90.00 |
Refinement procedure
| Resolution | 45.700 - 1.460 |
| R-factor | 0.1764 |
| Rwork | 0.175 |
| R-free | 0.20840 |
| Structure solution method | AB INITIO PHASING |
| RMSD bond length | 0.009 |
| RMSD bond angle | 0.993 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | Arcimboldo |
| Refinement software | PHENIX ((dev_4788: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 45.700 | 1.490 |
| High resolution limit [Å] | 1.460 | 1.460 |
| Rmerge | 0.089 | 0.822 |
| Rmeas | 0.096 | 0.957 |
| Rpim | 0.036 | 0.478 |
| Number of reflections | 43928 | 1925 |
| <I/σ(I)> | 13.19 | 1.46 |
| Completeness [%] | 94.9 | 62.72 |
| Redundancy | 6.7 | 3.8 |
| CC(1/2) | 0.997 | 0.517 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 8 | 293.15 | 1.5M NaCl, 0.1M Sodium Acetate pH4.5 |
