9EQK
WWP1 WW2-2,3-linker-WW3-WW4-HECT (WWP1-2L34H) with ordered WW2 domain
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | DIAMOND BEAMLINE I24 |
Synchrotron site | Diamond |
Beamline | I24 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-02-05 |
Detector | DECTRIS EIGER2 X CdTe 9M |
Wavelength(s) | 0.6199 |
Spacegroup name | C 1 2 1 |
Unit cell lengths | 226.984, 59.719, 108.258 |
Unit cell angles | 90.00, 99.41, 90.00 |
Refinement procedure
Resolution | 84.490 - 3.000 |
R-factor | 0.2089 |
Rwork | 0.205 |
R-free | 0.27440 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.189 |
Data reduction software | autoPROC |
Data scaling software | autoPROC |
Phasing software | PHASER |
Refinement software | PHENIX (1.20.1_4487) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 106.823 | 8.605 |
High resolution limit [Å] | 3.000 | 3.171 |
Rmerge | 0.200 | |
Rmeas | 0.420 | |
Rpim | 0.159 | |
Number of reflections | 29046 | 1181 |
<I/σ(I)> | 4.7 | |
Completeness [%] | 94.5 | 100 |
Redundancy | 6.8 | 7 |
CC(1/2) | 0.975 | 0.368 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 6.5 | 289 | 100 mM Tris.HCl pH 6.5, 17.5 % reagent alcohol (90 % ethanol, 5 % methanol, 5 % isopropanol). |