9EIB
Structure of Myroides odoratus prophage anti-Thoeris 2 (ModTad2) in complex with hisADPR
Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | NSLS-II BEAMLINE 17-ID-2 |
| Synchrotron site | NSLS-II |
| Beamline | 17-ID-2 |
| Temperature [K] | 80 |
| Detector technology | PIXEL |
| Collection date | 2024-06-20 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.97934 |
| Spacegroup name | P 63 2 2 |
| Unit cell lengths | 92.692, 92.692, 78.079 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 30.340 - 1.670 |
| R-factor | 0.2093 |
| Rwork | 0.208 |
| R-free | 0.23720 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.007 |
| RMSD bond angle | 1.011 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.21_5207) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 30.341 | 1.783 |
| High resolution limit [Å] | 1.668 | 1.668 |
| Rpim | 0.032 | |
| Number of reflections | 16652 | 834 |
| <I/σ(I)> | 15 | |
| Completeness [%] | 100.0 | 58.9 |
| Redundancy | 38.9 | |
| CC(1/2) | 0.783 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 291 | 0.1 M CH3COONa pH 4.4 and 24% PEG-4000 |
