9EHN

Co-MAHF-9 A8T Metal Alpha-Helix Framework

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	SYNCHROTRON
Source details	MAX IV BEAMLINE BioMAX
Synchrotron site	MAX IV
Beamline	BioMAX
Temperature [K]	100
Detector technology	PIXEL
Collection date	2024-05-08
Detector	DECTRIS EIGER X 16M
Wavelength(s)	0.68879
Spacegroup name	P 1
Unit cell lengths	16.470, 21.720, 23.650
Unit cell angles	103.64, 109.38, 108.91

Refinement procedure

Resolution	18.970 - 0.980
R-factor	0.1668
Rwork	0.165
R-free	0.18390
Structure solution method	MOLECULAR REPLACEMENT
RMSD bond length	0.011
RMSD bond angle	1.916
Data reduction software	XDS
Data scaling software	XDS
Phasing software	PHASER
Refinement software	PHENIX (1.20.1_4487)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	18.970	1.015
High resolution limit [Å]	0.980	0.980
Number of reflections	15329	1463
<I/σ(I)>	5.29
Completeness [%]	98.8
Redundancy	6.3
CC(1/2)	0.991	0.939

Crystallization Conditions

crystal ID	method	pH	temperature	details
1	SLOW COOLING		298	water, acetonitrile, cobalt acetate, methanol
1	SLOW COOLING		298	water, acetonitrile, cobalt acetate, methanol