Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2022-05-23 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.9179 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 115.540, 55.030, 93.030 |
| Unit cell angles | 90.00, 103.17, 90.00 |
Refinement procedure
| Resolution | 56.250 - 2.420 |
| R-factor | 0.2073 |
| Rwork | 0.205 |
| R-free | 0.24220 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.002 |
| RMSD bond angle | 0.503 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 56.250 | 2.507 |
| High resolution limit [Å] | 2.420 | 2.420 |
| Number of reflections | 21861 | 2189 |
| <I/σ(I)> | 4.88 | |
| Completeness [%] | 99.3 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.958 | 0.828 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 296 | 20% PEG 3350, 0.2M Lithium Nitrate |
