Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-04-19 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1.0 |
| Spacegroup name | P 1 21 1 |
| Unit cell lengths | 55.068, 98.956, 59.102 |
| Unit cell angles | 90.00, 107.50, 90.00 |
Refinement procedure
| Resolution | 46.390 - 1.860 |
| R-factor | 0.1631 |
| Rwork | 0.161 |
| R-free | 0.20600 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.012 |
| RMSD bond angle | 1.140 |
| Data reduction software | autoPROC |
| Data scaling software | autoPROC |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.21.1_5286) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 46.390 | 1.928 |
| High resolution limit [Å] | 1.860 | 1.862 |
| Number of reflections | 50064 | 4977 |
| <I/σ(I)> | 10.7 | |
| Completeness [%] | 99.0 | |
| Redundancy | 3.5 | |
| CC(1/2) | 0.997 | 0.880 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 296 | 20% PEG 3350, 0.1M Bis-Tris Propane pH 6.5, 0.2M Sodium Acetate |
