9DKZ

In situ microED structure of the Eosinophil major basic protein-1

Experimental procedure

Spacegroup name	P 2 21 21
Unit cell lengths	31.240, 57.870, 59.060
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	28.930 - 3.200
R-factor	0.2727
Rwork	0.268
R-free	0.31100
RMSD bond length	0.005
RMSD bond angle	1.043
Data reduction software	XDS (Jun 30, 2023 BUILT=20230630)
Data scaling software	XSCALE (Jun 30, 2023 BUILT=20230630)
Phasing software	PHASER (2.8.3)
Refinement software	PHENIX (1.21.1_5286)

Data quality characteristics

	Overall	Inner shell	Outer shell
Low resolution limit [Å]			3.290
High resolution limit [Å]	3.200	13.950	3.200
Rmerge	0.690	0.326	4.130
Rmeas	0.719	0.353	4.290
Total number of observations	24817
Number of reflections	1912	30	150
<I/σ(I)>	3.2	4.14	0.81
Completeness [%]	96.1
CC(1/2)	0.931	0.969	0.559