Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | ALS BEAMLINE 5.0.2 |
| Synchrotron site | ALS |
| Beamline | 5.0.2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2020-12-08 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 0.99984 |
| Spacegroup name | C 1 2 1 |
| Unit cell lengths | 97.111, 81.942, 54.831 |
| Unit cell angles | 90.00, 117.11, 90.00 |
Refinement procedure
| Resolution | 48.807 - 1.549 |
| Rwork | 0.225 |
| R-free | 0.25100 |
| Structure solution method | MOLECULAR REPLACEMENT |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | PRIME-X |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 48.807 | 1.576 |
| High resolution limit [Å] | 1.549 | 1.549 |
| Rmerge | 0.038 | 1.036 |
| Rmeas | 0.043 | 1.194 |
| Rpim | 0.021 | 0.584 |
| Number of reflections | 54559 | 2691 |
| <I/σ(I)> | 15.373 | 1.396 |
| Completeness [%] | 98.4 | 97.71 |
| Redundancy | 4.18 | 3.97 |
| CC(1/2) | 0.999 | 0.726 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 293 | 0.1 M bis-tris pH 6.5, 32% (w/v) polyethylene glycol 2000 monomethyl ether |
