Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | ALBA BEAMLINE XALOC |
Synchrotron site | ALBA |
Beamline | XALOC |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2021-06-10 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.97926 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 62.703, 62.703, 149.792 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 48.124 - 2.468 |
Rwork | 0.186 |
R-free | 0.26270 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.007 |
RMSD bond angle | 1.712 |
Data reduction software | XDS |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | REFMAC (5.8.0425) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.620 |
High resolution limit [Å] | 2.468 | 2.468 |
Number of reflections | 11390 | 1783 |
<I/σ(I)> | 13.07 | 1.45 |
Completeness [%] | 99.9 | |
Redundancy | 15.9 | |
CC(1/2) | 0.910 | 0.910 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 293 | 0.1 M Bis-Tris-Propane, pH 9.0, 10% PEG 20,000 |