Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | APS BEAMLINE 17-ID |
| Synchrotron site | APS |
| Beamline | 17-ID |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2018-02-02 |
| Detector | DECTRIS PILATUS 6M |
| Wavelength(s) | 1 |
| Spacegroup name | P 21 21 2 |
| Unit cell lengths | 93.104, 130.170, 35.923 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 16.400 - 1.950 |
| R-factor | 0.308 |
| Rwork | 0.307 |
| R-free | 0.33400 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.008 |
| RMSD bond angle | 0.960 |
| Data reduction software | XDS |
| Data scaling software | Aimless |
| Phasing software | PHASER |
| Refinement software | BUSTER (2.11.8 (20-OCT-2021)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 75.730 | 2.220 |
| High resolution limit [Å] | 1.950 | 1.960 |
| Rmerge | 0.100 | 0.558 |
| Number of reflections | 21574 | 1079 |
| <I/σ(I)> | 10.8 | 1.7 |
| Completeness [%] | 91.7 | 49.2 |
| Redundancy | 5.3 | 2.5 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 295 | 0.1 M tri-sodium citrate dihydrate pH 5.6, 20% (w/v) PEG 4,000, 20% (v/v) isopropanol |
