9CGT

STRUCTURE OF CYCLODEXTRIN GLYCOSYLTRANSFERASE COMPLEXED WITH A THIO-MALTOPENTAOSE

Experimental procedure

Experimental method	SINGLE WAVELENGTH
Source type	ROTATING ANODE
Source details	RIGAKU RU200
Temperature [K]	298
Detector technology	AREA DETECTOR
Collection date	1996-11-01
Detector	SIEMENS
Spacegroup name	P 21 21 21
Unit cell lengths	94.600, 104.700, 113.600
Unit cell angles	90.00, 90.00, 90.00

Refinement procedure

Resolution	30.000 - 2.500
R-factor	0.147
Rwork	0.147
R-free	0.18200
Structure solution method	OTHER
RMSD bond length	0.010
RMSD bond angle	1.300
Data reduction software	XDS
Data scaling software	XDS
Refinement software	X-PLOR (3.851)

Data quality characteristics

	Overall	Outer shell
Low resolution limit [Å]	33.361	2.270
High resolution limit [Å]	2.218	2.220
Number of reflections	42320
<I/σ(I)>	17	6.1
Completeness [%]	75.1	19.3
Redundancy	2.2	1

Crystallization Conditions

crystal ID	method	pH	temperature	details
1		6.9		pH 6.9