Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | ROTATING ANODE |
| Source details | RIGAKU MICROMAX-002 |
| Temperature [K] | 120 |
| Detector technology | PIXEL |
| Collection date | 2023-01-24 |
| Detector | Bruker PHOTON II |
| Wavelength(s) | 1.54301 |
| Spacegroup name | I 1 2 1 |
| Unit cell lengths | 51.768, 81.474, 90.380 |
| Unit cell angles | 90.00, 96.83, 90.00 |
Refinement procedure
| Resolution | 24.610 - 1.800 |
| R-factor | 0.2178 |
| Rwork | 0.216 |
| R-free | 0.26010 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.009 |
| RMSD bond angle | 1.093 |
| Data reduction software | PROTEUM PLUS |
| Data scaling software | Aimless |
| Phasing software | PHENIX |
| Refinement software | PHENIX (1.18.2_3874) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 24.610 | 1.864 |
| High resolution limit [Å] | 1.800 | 1.800 |
| Rmerge | 0.128 | 0.878 |
| Rmeas | 0.133 | 0.943 |
| Rpim | 0.037 | 0.340 |
| Number of reflections | 34512 | 3425 |
| <I/σ(I)> | 10.8 | 1.36 |
| Completeness [%] | 99.7 | 99.53 |
| Redundancy | 11.5 | |
| CC(1/2) | 0.997 | 0.778 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, HANGING DROP | 289 | 0.2 M Ammonium phosphate dibasic, 17% W/v PEG3350, pH8.0 |
