Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SLS BEAMLINE X06SA |
| Synchrotron site | SLS |
| Beamline | X06SA |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2019-09-23 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 1 |
| Spacegroup name | P 32 2 1 |
| Unit cell lengths | 90.781, 90.781, 122.616 |
| Unit cell angles | 90.00, 90.00, 120.00 |
Refinement procedure
| Resolution | 78.620 - 1.440 |
| R-factor | 0.14351 |
| Rwork | 0.142 |
| R-free | 0.17007 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.013 |
| RMSD bond angle | 1.667 |
| Data reduction software | XDS |
| Data scaling software | XSCALE |
| Phasing software | PHASER |
| Refinement software | REFMAC (5.8.0155) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 78.620 | 1.690 |
| High resolution limit [Å] | 1.440 | 1.440 |
| Rmerge | 0.035 | 0.483 |
| Rmeas | 0.041 | 0.567 |
| Number of reflections | 104088 | 39885 |
| <I/σ(I)> | 17.77 | 2.8 |
| Completeness [%] | 98.3 | 99.7 |
| Redundancy | 3.6 | 3.6 |
| CC(1/2) | 0.999 | 0.839 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION | 293 | 0.10 M NaAcetate pH 4.8, 2.0 M (NH4)2SO4, 30 % Glycerol |
