8IL5
Crystal structure of alcohol oxidase PcAOX(M59V/Q60P/R61N)(Phanerochaete chrysosporium)
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL19U1 |
Synchrotron site | SSRF |
Beamline | BL19U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2022-10-02 |
Detector | DECTRIS PILATUS3 6M |
Wavelength(s) | 0.9769 |
Spacegroup name | P 4 21 2 |
Unit cell lengths | 161.260, 161.260, 113.340 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 23.182 - 2.500 |
R-factor | 0.168335889111 |
Rwork | 0.166 |
R-free | 0.21340 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.009 |
RMSD bond angle | 1.309 |
Data reduction software | HKL-2000 |
Phasing software | PHASER |
Refinement software | PHENIX (1.9_1692+SVN) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 24.010 | 2.520 |
High resolution limit [Å] | 2.460 | 2.460 |
Number of reflections | 54647 | 3996 |
<I/σ(I)> | 14.9 | |
Completeness [%] | 99.9 | |
Redundancy | 51 | |
CC(1/2) | 0.998 | 0.720 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, HANGING DROP | 290 | 1.6 M ammonium sulfate, 0.1M MES pH 6.5, 10% (v/v) 1,4-Dioxane |