8ZLZ
The complex crystal structure of CcmS and C-terminus of CcmK1.
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL18U1 |
Synchrotron site | SSRF |
Beamline | BL18U1 |
Temperature [K] | 100 |
Detector technology | PIXEL |
Collection date | 2024-04-07 |
Detector | DECTRIS PILATUS 6M |
Wavelength(s) | 0.9785 |
Spacegroup name | P 41 21 2 |
Unit cell lengths | 67.493, 67.493, 118.108 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 34.010 - 1.670 |
R-factor | 0.1845 |
Rwork | 0.182 |
R-free | 0.21720 |
Structure solution method | MOLECULAR REPLACEMENT |
RMSD bond length | 0.010 |
RMSD bond angle | 1.145 |
Data reduction software | autoPROC |
Data scaling software | Aimless |
Phasing software | PHASER |
Refinement software | PHENIX ((1.20.1_4487: ???)) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 58.600 | 1.760 |
High resolution limit [Å] | 1.670 | 1.670 |
Number of reflections | 32268 | 4199 |
<I/σ(I)> | 27.8 | |
Completeness [%] | 98.5 | |
Redundancy | 22 | |
CC(1/2) | 0.999 | 0.842 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 291.15 | 0.2 M Lithium sulfate, 0.1 M TRIS pH8.5, 1.26 M Ammonium sulfate |