Experimental procedure
| Experimental method | SINGLE WAVELENGTH |
| Source type | SYNCHROTRON |
| Source details | SSRF BEAMLINE BL10U2 |
| Synchrotron site | SSRF |
| Beamline | BL10U2 |
| Temperature [K] | 100 |
| Detector technology | PIXEL |
| Collection date | 2021-07-21 |
| Detector | DECTRIS EIGER X 16M |
| Wavelength(s) | 0.987 |
| Spacegroup name | P 21 21 21 |
| Unit cell lengths | 68.512, 82.323, 101.167 |
| Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
| Resolution | 52.660 - 1.930 |
| R-factor | 0.1818 |
| Rwork | 0.180 |
| R-free | 0.20900 |
| Structure solution method | MOLECULAR REPLACEMENT |
| RMSD bond length | 0.011 |
| RMSD bond angle | 1.067 |
| Refinement software | PHENIX ((1.19.2_4158: ???)) |
Data quality characteristics
| Overall | Outer shell | |
| Low resolution limit [Å] | 52.660 | 2.003 |
| High resolution limit [Å] | 1.930 | 1.934 |
| Number of reflections | 41305 | 4265 |
| <I/σ(I)> | 9.7 | |
| Completeness [%] | 94.9 | |
| Redundancy | 2 | |
| CC(1/2) | 0.995 | 0.708 |
Crystallization Conditions
| crystal ID | method | pH | temperature | details |
| 1 | VAPOR DIFFUSION, SITTING DROP | 298.15 | 39.3% ethylene glycol 0.1M MES, pH5.6 200mM Zn(OAc)2 |
