8Z5J
Beta-catenin Crystal Structure
Experimental procedure
Experimental method | SINGLE WAVELENGTH |
Source type | SYNCHROTRON |
Source details | SSRF BEAMLINE BL17U1 |
Synchrotron site | SSRF |
Beamline | BL17U1 |
Temperature [K] | 293 |
Detector technology | PIXEL |
Collection date | 2016-07-14 |
Detector | DECTRIS EIGER X 16M |
Wavelength(s) | 0.9791 |
Spacegroup name | C 2 2 21 |
Unit cell lengths | 63.850, 103.150, 185.640 |
Unit cell angles | 90.00, 90.00, 90.00 |
Refinement procedure
Resolution | 50.000 - 2.800 |
R-factor | 0.224 |
Rwork | 0.198 |
R-free | 0.26400 |
Structure solution method | FOURIER SYNTHESIS |
Data reduction software | HKL-2000 (4.5) |
Data scaling software | HKL-2000 (4.5) |
Phasing software | PHASES (1.2) |
Refinement software | REFMAC (5.5) |
Data quality characteristics
Overall | Outer shell | |
Low resolution limit [Å] | 50.000 | 2.900 |
High resolution limit [Å] | 2.800 | 2.800 |
Number of reflections | 18454 | 14764 |
<I/σ(I)> | 26.5 | |
Completeness [%] | 92.5 | 86 |
Redundancy | 7.3 | |
CC(1/2) | 0.980 | 0.980 |
Crystallization Conditions
crystal ID | method | pH | temperature | details |
1 | VAPOR DIFFUSION, SITTING DROP | 7.5 | 277 | 14% PEG 3350, 0.1M Hepes pH 7.5, 0.2M L-proline, 20% glycerol |